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Freeze Dryers

 

 

 

Research Series

 

System features:

 

• PC/PLC Control Standard
• -53C or -855C Condenser Temperature
• 30L Condenser Capacity
• Remote Condenser with Hot Gas Defrost
• From 1 to 5 Shelves in Bulk or Stoppering
• -48C or -70C Shelf Temperature
• Fluid Filled Hollow Shelves, 12"x 24" Each
• Rectangular 316L Chamber
• Hydraulic Stoppering
• Pirani Pressure Control and Gas Backfill 

  Standard
• Optional Manifold

 

System performance:

 

Shelf pull down from +20 to -40C in less than 30minutes

Temperature resolution 0.1 C

Vacuum pull down to 100 mT in less than 15 minutes

Vacuum leak rate less than 30 mT per hour

Achieves vacuum level of 5 mT in clean dry systems

 

 

 

Research Series is a new generation laboratory research freeze dryer that is both a shelf and manifold dryer. Product can be loaded on the shelves and frozen prior to drying or can be frozen  in an optional shell freezer for manifold drying. A rectangular chamber offers a compact profile with either stoppering or bulk assembly. Hydraulic stoppering is provided by a bottom up hydraulic cylinder. Both options have a radiant heat plate above the top shelf for uniform drying on all shelves. All internal surfaces are constructed of 316L stainless steel and offer a polish of 20 Ra or better. A coil condenser is located between the product and the vacuum pump providing maximum condensing surface area and vacuum pump protection. A 4" vapor port connects the two chambers, with a 6" option. An isolation valve can be added for end of drying testing. Hot gas is used for defrosting the condenser when drying is complete.
Fluid filled hollow shelves with a serpentine fluid path provide the most uniform shelf temperature possible resulting in consistent and repeatable drying. All units come with one product tray per shelf, either a removable bottom or bulk.

Options include a Shelf Latching Kit, Isolation Valve, Capacitance Manometer, Moisture Sensor, Clean Room Configuration, Sample Extractor, 6"/8" vapor ports.

 

Specifications:

 

Model

RD 53

RD 85

Condenser
Temp

-53 C

-85 C

Condenser
Capacity

20 liters/24 hours (30 liters max.)

Shelf Temperature

-48 C to +65 C

-70 C to +65 C

Refrigeration

3.5 HP Scroll
CFC-Free

3.5 HP and 2 HP
CFC-Free

Defrost

Hot  Gas - Automatic

Vacuum Pump

400 l / min.

Cabinet
Dimensions

35"W x 42"D x 73" H

Voltage

208-240V, 50/60Hz,
1PH, 20A

 

 

All the freeze dryers are built to meet the most exacting current Good Manufacturing Practices (cGMP) standards.

 

 

Shelves

Area
sq ft/sq m

Clearance
in/mm

1
2
3
4
5

2/.186
4/.373
6/.559
8/.746
10/.932

11.5/292
5.5/139
3.5/89
2.5/63
1.9/48

 

 

Opti-Dry™ Control Features

 

Automatic

10 Freezing Steps
16 Drying Steps with Pressure Control
1 Step Secondary and 1 Step Final Drying
Alarms, Recipe Management, Data Logging

 

 

 

Maintenance

 

Independent Operation of Components, with
Troubleshooting and Calibration

Manual

 

Individual Switches for Shelf, Condenser, Vacuum, Control, Isolation Valve, and Release. Single Set-points for Shelf and Vacuum.

 

 

Opti-Dry (TM)
Plus Features

 Includes Opti-Dry Basic features
 Eutectic Point Determination
 Product temperature feedback
 Optimizes the recipe, both freezing and primary drying, based on the product temperature avg.

System Test

 

Performance Evaluation of Shelf,
Condenser, Vacuum, Heating, and Control

Opti-Dry (TM)
Pro Features

 Includes Opti-Dry Basic & Opti-Dry Plus features
 Primary Drying Endpoint   

 Determination Via:   Pirani/Capacitance Manometer Comparison

Defrost

 Automatic Timed Hot Gas

Leak Rate

Automatic Testing of System Performance

 

 

 

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